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Iodine-Promoted C(spĀ²)--H Thiolation of Maleimides with Dimethyl Sulfoxide and Thiols.
- Source :
- Synthesis; 2018, Vol. 50 Issue 20, p4113-4123, 11p
- Publication Year :
- 2018
-
Abstract
- Iodine-promoted C(sp²)--H methylthiolation of maleimides using DMSO as synthon has been developed to afford 3-methylthiomaleimides in moderate yields under metal-free conditions. In addition, 3-thiomaleimides were synthesized from maleimides and thiols in the presence of iodine and triethylamine. The methods are simple and efficient for the formation of C--S bond. [ABSTRACT FROM AUTHOR]
- Subjects :
- IODINE
CARBON-hydrogen bonds
MALEIMIDES
DIMETHYL sulfoxide
THIOLS
Subjects
Details
- Language :
- English
- ISSN :
- 00397881
- Volume :
- 50
- Issue :
- 20
- Database :
- Complementary Index
- Journal :
- Synthesis
- Publication Type :
- Academic Journal
- Accession number :
- 132099599
- Full Text :
- https://doi.org/10.1055/s-0037-1609585