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Synthesis and Characterization of Acetic Acid and Ethanoic Acid (based)-Maleimide.

Authors :
Poad, Siti Nashwa Mohd
Hassan, Nurul Izzaty
Hassan, Nur Hasyareeda
Source :
AIP Conference Proceedings; 2016, Vol. 1784 Issue 1, p1-7, 7p, 2 Diagrams, 3 Graphs
Publication Year :
2016

Abstract

A new route to the synthesis of maleimide is described. 2-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1- yl)acetic acid maleimide (1) and 2-(4-(2,5-Dioxo-2,5-dihydro- 1H-pyrrol-1-yl)phenyl)ethanoic acid maleimide (2) have been synthesized by the reaction of maleic anhydride with glycine and 4-aminophenyl acetic aicd. Maleimide (1) was synthesized by conventional technique while maleimide (2) was synthesized by microwave method. The compounds were characterized using FT-Infrared (FT-IR), ¹H and <superscript>13</superscript>C Nuclear Magnetic Resonance (NMR) spectroscopies and Mass Spectrometry. [ABSTRACT FROM AUTHOR]

Details

Language :
English
ISSN :
0094243X
Volume :
1784
Issue :
1
Database :
Complementary Index
Journal :
AIP Conference Proceedings
Publication Type :
Conference
Accession number :
119585606
Full Text :
https://doi.org/10.1063/1.4966754