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Influence of Obtaining Conditions on Kinetics of the Initial Sintering Stage of Zirconia Nanopowders.
- Source :
- Nanoscale Research Letters; 5/4/2016, Vol. 11 Issue 1, p1-6, 6p
- Publication Year :
- 2016
-
Abstract
- The present paper is devoted to the problem of sintering ceramics based on yttria-stabilized zirconia (Y-TZP). In this paper, we studied the effect of two obtaining methods (co-precipitation and technical hydrolysis) on sintering kinetics of Y-TZP nanopowders. We used the constant rate of heating (CRH) method at different heating rates for determining the sintering mechanisms. The basic mechanism and activation energy ( Q) of diffusion at the initial sintering stage were estimated using the sintering rate equations that are applicable to the CRH data. We found that nanopowder 3Y-TZP produced by the co-precipitation method (DIPE) was sintered according to the volume diffusion mechanism ( n = 1/2) and nanopowder TZ-3Y (TOSOH) produced by the technical hydrolysis was sintered according to the grain boundary diffusion mechanism ( n = 1/3). [ABSTRACT FROM AUTHOR]
Details
- Language :
- English
- ISSN :
- 19317573
- Volume :
- 11
- Issue :
- 1
- Database :
- Complementary Index
- Journal :
- Nanoscale Research Letters
- Publication Type :
- Academic Journal
- Accession number :
- 115097817
- Full Text :
- https://doi.org/10.1186/s11671-016-1452-3