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The stability of Tenax TA thermal desorption tubes in simulated field conditions on the HAPSITE ER.

Authors :
Harshman, Sean W.
Dershem, Victoria L.
Fan, Maomian
Watts, Brandy S.
Slusher, Grant M.
Flory, Laura E.
Grigsby, Claude C.
Ott, Darrin K.
Source :
International Journal of Environmental Analytical Chemistry; Sep2015, Vol. 95 Issue 11, p1014-1029, 16p
Publication Year :
2015

Abstract

Due to the growing need to monitor aircraft cabin, cockpit and breathing-line air quality, functional assessment of sampling equipment for the specialised field conditions of flight need to be established for both in-flight and ground safety. In this article, we assess the reliability of Tenax TA thermal desorption tubes to perform under various relevant field sampling conditions, such as storage temperature, loading temperature, vibrational velocity, gravitational force (G Force) and altitude pressure with semi-real-time gas chromatograph-mass spectrometer (GC-MS) analysis on the field portable HAPSITE®ER (Hazardous Air Pollutants on Site Extended Range) instrument. First, we show that Tenax TA thermal desorption tubes can handle storage under extreme environmental conditions, 4–77°C, over numerous analytical test cycles. Next, we confirm that extreme loading temperature, both hot (77°C) and cold (4°C), does not affect the analytical reliability of Tenax TA thermal desorption tubes. Then, we illustrate that G Force may have a significant (p ≤ 0.0364) effect on Tenax TA performance while vibrational velocity (p ≤ 0.7265) and low ambient air pressure (p ≤ 0.1753), such as that found at high altitude, do not. Finally, several Tenax TA thermal desorption tubes were flight-tested, demonstrating that the durability of these tubes maybe insufficient for use on military cargo aircraft (p = 0.0107). The results presented here provide a rationale for additional testing of Tenax TA thermal desorption tubes for flight suitability. [ABSTRACT FROM PUBLISHER]

Details

Language :
English
ISSN :
03067319
Volume :
95
Issue :
11
Database :
Complementary Index
Journal :
International Journal of Environmental Analytical Chemistry
Publication Type :
Academic Journal
Accession number :
109463779
Full Text :
https://doi.org/10.1080/03067319.2015.1077520