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The XFM beamline at the Australian Synchrotron.

Authors :
Howard DL
de Jonge MD
Afshar N
Ryan CG
Kirkham R
Reinhardt J
Kewish CM
McKinlay J
Walsh A
Divitcos J
Basten N
Adamson L
Fiala T
Sammut L
Paterson DJ
Source :
Journal of synchrotron radiation [J Synchrotron Radiat] 2020 Sep 01; Vol. 27 (Pt 5), pp. 1447-1458. Date of Electronic Publication: 2020 Aug 19.
Publication Year :
2020

Abstract

The X-ray fluorescence microscopy (XFM) beamline is an in-vacuum undulator-based X-ray fluorescence (XRF) microprobe beamline at the 3 GeV Australian Synchrotron. The beamline delivers hard X-rays in the 4-27 keV energy range, permitting K emission to Cd and L and M emission for all other heavier elements. With a practical low-energy detection cut-off of approximately 1.5 keV, low-Z detection is constrained to Si, with Al detectable under favourable circumstances. The beamline has two scanning stations: a Kirkpatrick-Baez mirror microprobe, which produces a focal spot of 2 µm × 2 µm FWHM, and a large-area scanning `milliprobe', which has the beam size defined by slits. Energy-dispersive detector systems include the Maia 384, Vortex-EM and Vortex-ME3 for XRF measurement, and the EIGER2 X 1 Mpixel array detector for scanning X-ray diffraction microscopy measurements. The beamline uses event-mode data acquisition that eliminates detector system time overheads, and motion control overheads are significantly reduced through the application of an efficient raster scanning algorithm. The minimal overheads, in conjunction with short dwell times per pixel, have allowed XFM to establish techniques such as full spectroscopic XANES fluorescence imaging, XRF tomography, fly scanning ptychography and high-definition XRF imaging over large areas. XFM provides diverse analysis capabilities in the fields of medicine, biology, geology, materials science and cultural heritage. This paper discusses the beamline status, scientific showcases and future upgrades.

Details

Language :
English
ISSN :
1600-5775
Volume :
27
Issue :
Pt 5
Database :
MEDLINE
Journal :
Journal of synchrotron radiation
Publication Type :
Academic Journal
Accession number :
32876622
Full Text :
https://doi.org/10.1107/S1600577520010152