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Copper-catalysed three-component carboiodination of arynes: expeditious synthesis of o-alkynyl aryl iodides.

Authors :
Cao W
Niu SL
Shuai L
Xiao Q
Source :
Chemical communications (Cambridge, England) [Chem Commun (Camb)] 2020 Jan 18; Vol. 56 (6), pp. 972-975. Date of Electronic Publication: 2019 Dec 20.
Publication Year :
2020

Abstract

A copper-catalysed three-component iodoalkynylation reaction of arynes for the expeditious and versatile synthesis of o-alkynyl aryl iodides has been developed. Mechanism research shows that the reaction goes through two steps enabled by copper catalysis: the formation of 1-iodo-2-arylacetylene and the insertion of the aryne into a C(sp)-I bond.

Details

Language :
English
ISSN :
1364-548X
Volume :
56
Issue :
6
Database :
MEDLINE
Journal :
Chemical communications (Cambridge, England)
Publication Type :
Academic Journal
Accession number :
31859294
Full Text :
https://doi.org/10.1039/c9cc09160b