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The Dresden in-situ (S)TEM special with a continuous-flow liquid-helium cryostat.

Authors :
Börrnert F
Kern F
Harder F
Riedel T
Müller H
Büchner B
Lubk A
Source :
Ultramicroscopy [Ultramicroscopy] 2019 Aug; Vol. 203, pp. 12-20. Date of Electronic Publication: 2019 Feb 08.
Publication Year :
2019

Abstract

Fundamental solid state physics phenomena often occur at very low temperatures, requiring liquid helium cooling in experimental studies. Transmission electron microscopy is a well-established characterization method, which allows probing crucial materials properties down to nanometre and even atomic resolution. Due to the limited space in the object plane, however, suitable liquid-helium cooling is very challenging. To overcome this limitation, resolving power was sacrificed in our Dresden in-situ (S)TEM special, resulting in more than 60 mm usable experimental space in all directions with the specimen in the centre. With the installation of a continuous-flow liquid-helium cryostat, any temperature between 6.5 K and 400 K can be set precisely and kept for days. The information limit of the Dresden in-situ (S)TEM special is about 5 nm. It is shown that the resolution of the Dresden in-situ (S)TEM special is currently not limited by aberrations, but by external instabilities.<br /> (Copyright © 2019 Elsevier B.V. All rights reserved.)

Details

Language :
English
ISSN :
1879-2723
Volume :
203
Database :
MEDLINE
Journal :
Ultramicroscopy
Publication Type :
Academic Journal
Accession number :
30902417
Full Text :
https://doi.org/10.1016/j.ultramic.2019.01.005