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The Dresden in-situ (S)TEM special with a continuous-flow liquid-helium cryostat.
- Source :
-
Ultramicroscopy [Ultramicroscopy] 2019 Aug; Vol. 203, pp. 12-20. Date of Electronic Publication: 2019 Feb 08. - Publication Year :
- 2019
-
Abstract
- Fundamental solid state physics phenomena often occur at very low temperatures, requiring liquid helium cooling in experimental studies. Transmission electron microscopy is a well-established characterization method, which allows probing crucial materials properties down to nanometre and even atomic resolution. Due to the limited space in the object plane, however, suitable liquid-helium cooling is very challenging. To overcome this limitation, resolving power was sacrificed in our Dresden in-situ (S)TEM special, resulting in more than 60 mm usable experimental space in all directions with the specimen in the centre. With the installation of a continuous-flow liquid-helium cryostat, any temperature between 6.5 K and 400 K can be set precisely and kept for days. The information limit of the Dresden in-situ (S)TEM special is about 5 nm. It is shown that the resolution of the Dresden in-situ (S)TEM special is currently not limited by aberrations, but by external instabilities.<br /> (Copyright © 2019 Elsevier B.V. All rights reserved.)
Details
- Language :
- English
- ISSN :
- 1879-2723
- Volume :
- 203
- Database :
- MEDLINE
- Journal :
- Ultramicroscopy
- Publication Type :
- Academic Journal
- Accession number :
- 30902417
- Full Text :
- https://doi.org/10.1016/j.ultramic.2019.01.005