Back to Search
Start Over
Synthesis and Characterization of Nanoscale Tungsten Particles with Hollow Superstructure Using Spray Drying Combined with Calcination Process.
- Source :
-
Nanoscale research letters [Nanoscale Res Lett] 2019 Feb 26; Vol. 14 (1), pp. 68. Date of Electronic Publication: 2019 Feb 26. - Publication Year :
- 2019
-
Abstract
- Nanoscale tungsten (W) powder is used in some special materials. In this study, a hollow superstructure W powder consisting of nanoparticles was synthesized by spray drying combined with two-step calcination from commercial (NH <subscript>4</subscript> ) <subscript>6</subscript> W <subscript>7</subscript> O <subscript>24</subscript> ·6H <subscript>2</subscript> O. The high-pressure gas (HPG) was the significant factor in spray drying process, which affect the BET surface area and average particles size of the spray-dried powders. The detailed influences of calcined steps and calcination temperature in the microstructure and average particles size of final W particles were investigated. The size distribution of as-synthesized nanoscale W particles with hollow superstructure was from 40 to 200 nm, and the average size was about 100 nm. The as-synthesized W powder shows good sintering properties. It should be noted that the powder technology in this study can be used to synthesize other powders with high-performance requirements. .
Details
- Language :
- English
- ISSN :
- 1931-7573
- Volume :
- 14
- Issue :
- 1
- Database :
- MEDLINE
- Journal :
- Nanoscale research letters
- Publication Type :
- Academic Journal
- Accession number :
- 30806833
- Full Text :
- https://doi.org/10.1186/s11671-019-2904-3