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Electric discharge machine for preparation of diamond anvil cell sample chambers.

Authors :
Proctor JE
Massey D
Source :
The Review of scientific instruments [Rev Sci Instrum] 2018 Oct; Vol. 89 (10), pp. 105109.
Publication Year :
2018

Abstract

We have designed and constructed a novel electric discharge machine designed primarily for the preparation of sample chambers in rhenium and stainless steel gaskets for diamond anvil cell experiments. Our design combines automatic stage movement with relatively low voltage (100 V) operation and routinely achieves a drilling/erosion speed of approximately 0.4 μ m s <superscript>-1</superscript> . The machine is used for preparing 100 μ m diameter sample chambers for diamond anvil cell experiments with 250 μ m culets and has also been used to prepare 50 μ m diameter sample chambers for diamond anvil cell experiments with 100 μ m culets to access a pressure of 165 GPa.

Details

Language :
English
ISSN :
1089-7623
Volume :
89
Issue :
10
Database :
MEDLINE
Journal :
The Review of scientific instruments
Publication Type :
Academic Journal
Accession number :
30399960
Full Text :
https://doi.org/10.1063/1.5050500