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Scalable Synthesis of Hydrido-Disiloxanes from Silanes: A One-Pot Preparation of 1,3-Diphenyldisiloxane from Phenylsilane.
- Source :
-
Synthesis [Synthesis (Stuttg)] 2018 Jan; Vol. 50 (2), pp. 278-281. Date of Electronic Publication: 2017 Sep 26. - Publication Year :
- 2018
-
Abstract
- A simple, one-pot, and high-yielding synthesis of 1,3-diphenyldisiloxane is presented. The preparation of similar symmetrical disiloxane materials is also accomplished with this same protocol. This mechano-chemical procedure is efficient and highly scalable, furnishing a convenient route to hydrido-disiloxanes from widely accessible commercially available silanes.
Details
- Language :
- English
- ISSN :
- 0039-7881
- Volume :
- 50
- Issue :
- 2
- Database :
- MEDLINE
- Journal :
- Synthesis
- Publication Type :
- Academic Journal
- Accession number :
- 29662252
- Full Text :
- https://doi.org/10.1055/s-0036-1588580