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ZnCl 2 Incorporated into Experimental Adhesives: Selected Physicochemical Properties and Resin-Dentin Bonding Stability.
- Source :
-
BioMed research international [Biomed Res Int] 2017; Vol. 2017, pp. 5940479. Date of Electronic Publication: 2017 Nov 15. - Publication Year :
- 2017
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Abstract
- The aim of this study was to evaluate the degree of conversion (DC%), water sorption (WS), solubility (SO), and resin-dentin bonding stability of experimental adhesive systems containing ZnCl <subscript>2</subscript> . Different concentrations (wt.%) of ZnCl <subscript>2</subscript> were added to a model etch-and-rinse adhesive system consisting of BISGMA, HEMA, UDMA, GDMA, water, and ethanol: Zn0 (0%-control group); Zn2 (2%); Zn3.5 (3.5%); and Zn5 (5%). Adper Single Bond 2 (SB) was used as commercial reference. The samples were light cured for 20s using a quartz-tungsten-halogen unit (650 mW/cm <superscript>2</superscript> ). DC% ( n = 5) was measured using FT-IR spectroscopy, and WS and SO ( n = 5) were calculated based on ISO4049. Microtensile bond strength ( μ TBS) and nanoleakage (NL) were measured after 24 h and 12 months of water storage ( n = 10). Data were analyzed using ANOVA and Tukey's HSD test (5%). Zn5 presented the lowest DC% and the highest WS and SO ( p < 0.05). Zn0 and Zn2 presented statistically similar DC%, WS, SO, and immediate μ TBS. All adhesives containing ZnCl <subscript>2</subscript> maintained a μ TBS stability after 12 months, but only Zn2 and Zn3.5 did not suffer an increase in NL. SB presented the highest immediate μ TBS but the greatest reduction after 12 months ( p < 0.05). The addition of 2 wt.% of ZnCl <subscript>2</subscript> in adhesive formulations seems to be a promising way to improve the resin-dentin bonding stability. Higher concentrations than 2 wt.% could impair some physicochemical properties.
- Subjects :
- Acid Etching, Dental methods
Chlorides therapeutic use
Dental Bonding instrumentation
Dental Cements therapeutic use
Dentin chemistry
Humans
Materials Testing
Resin Cements chemistry
Resin Cements therapeutic use
Resins, Synthetic therapeutic use
Tensile Strength
Zinc Compounds therapeutic use
Chlorides chemistry
Dental Cements chemistry
Resins, Synthetic chemistry
Zinc Compounds chemistry
Subjects
Details
- Language :
- English
- ISSN :
- 2314-6141
- Volume :
- 2017
- Database :
- MEDLINE
- Journal :
- BioMed research international
- Publication Type :
- Academic Journal
- Accession number :
- 29270433
- Full Text :
- https://doi.org/10.1155/2017/5940479