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Crystal structure of akuammicine, an indole alkaloid from Catharanthus roseus .

Authors :
Yahyazadeh M
Jerz G
Selmar D
Winterhalter P
Jones PG
Source :
Acta crystallographica. Section E, Crystallographic communications [Acta Crystallogr E Crystallogr Commun] 2017 Oct 20; Vol. 73 (Pt 11), pp. 1658-1661. Date of Electronic Publication: 2017 Oct 20 (Print Publication: 2017).
Publication Year :
2017

Abstract

The title compound, C <subscript>20</subscript> H <subscript>22</subscript> N <subscript>2</subscript> O <subscript>2</subscript> , an alkaloid isolated from the Madagascar periwinkle, crystallizes in P 1 with two independent but closely similar mol-ecules in the unit cell. The mol-ecules are linked into pairs by two N-H⋯O=C hydrogen bonds. The absolute configuration was confirmed by anomalous dispersion effects as S at the 3 and 15 positions, and R at the 7 position.

Details

Language :
English
ISSN :
2056-9890
Volume :
73
Issue :
Pt 11
Database :
MEDLINE
Journal :
Acta crystallographica. Section E, Crystallographic communications
Publication Type :
Academic Journal
Accession number :
29152344
Full Text :
https://doi.org/10.1107/S2056989017014529