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Short communication: Analysis of mycotoxins in Spanish milk.
- Source :
-
Journal of dairy science [J Dairy Sci] 2018 Jan; Vol. 101 (1), pp. 113-117. Date of Electronic Publication: 2017 Oct 18. - Publication Year :
- 2018
-
Abstract
- We surveyed the presence of 22 mycotoxins in 191 Spanish cow milk samples. Mycotoxins could be carried over from diet into animal milk and have toxic effects on human and animal health. The interaction of different mycotoxins may be additive or synergetic. Therefore, surveillance of mycotoxin co-occurrence in milk is recommended. Aflatoxins M <subscript>1</subscript> , B <subscript>1</subscript> , B <subscript>2</subscript> , G <subscript>1</subscript> , and G <subscript>2</subscript> , ochratoxins A and B, nivalenol, deoxynivalenol, deepoxy-deoxynivalenol, 3- and 15-acetyldeoxynivalenol, diacetoxyscirpenol, neosolaniol, fusarenon X, T-2 and HT-2 toxins, fumonisins B <subscript>1</subscript> , B <subscript>2</subscript> , and B <subscript>3</subscript> , sterigmatocystin, and zearalenone were analyzed. Samples were treated by liquid-liquid extraction with acidified acetonitrile, followed by an acetonitrile-water phase separation using sodium acetate. The analysis was carried out by HPLC coupled to a triple quadrupole mass spectrometer. None of the analyzed mycotoxins had a concentration level higher than their detection limit (0.05-10.1 µg/L). The aflatoxin M <subscript>1</subscript> in the samples never exceeded the level established by the European Union.<br /> (Copyright © 2018 American Dairy Science Association. Published by Elsevier Inc. All rights reserved.)
- Subjects :
- Aflatoxin B1 analysis
Animals
Cattle
Chromatography, High Pressure Liquid
Female
Fumonisins analysis
Limit of Detection
Ochratoxins analysis
Spain
T-2 Toxin analogs & derivatives
T-2 Toxin analysis
Tandem Mass Spectrometry
Trichothecenes analysis
Zearalenone analysis
Food Contamination analysis
Milk chemistry
Mycotoxins analysis
Subjects
Details
- Language :
- English
- ISSN :
- 1525-3198
- Volume :
- 101
- Issue :
- 1
- Database :
- MEDLINE
- Journal :
- Journal of dairy science
- Publication Type :
- Academic Journal
- Accession number :
- 29055539
- Full Text :
- https://doi.org/10.3168/jds.2017-13290