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Aberration measurement of the probe-forming system of an electron microscope using two-dimensional materials.

Authors :
Sawada H
Allen CS
Wang S
Warner JH
Kirkland AI
Source :
Ultramicroscopy [Ultramicroscopy] 2017 Nov; Vol. 182, pp. 195-204. Date of Electronic Publication: 2017 Jul 05.
Publication Year :
2017

Abstract

The geometric and chromatic aberration coefficients of the probe-forming system in an aberration corrected transmission electron microscope have been measured using a Ronchigram recorded from monolayer graphene. The geometric deformations within individual local angular sub-regions of the Ronchigram were analysed using an auto-correlation function and the aberration coefficients for the probe forming lens were calculated. This approach only requires the acquisition of a single Ronchigram allowing rapid measurement of the aberration coefficients. Moreover, the measurement precision for defocus and two-fold astigmatism is improved over that which can be achieved from analysis of Ronchigrams recorded from amorphous films. This technique can also be applied to aberration corrected STEM imaging of any hexagonal two-dimensional material.<br /> (Copyright © 2017 Elsevier B.V. All rights reserved.)

Details

Language :
English
ISSN :
1879-2723
Volume :
182
Database :
MEDLINE
Journal :
Ultramicroscopy
Publication Type :
Academic Journal
Accession number :
28709084
Full Text :
https://doi.org/10.1016/j.ultramic.2017.06.024