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Heteroacene Synthesis through C-S Cross-Coupling/5-endo-dig Cyclization.

Authors :
Oechsle P
Flörke U
Egold H
Paradies J
Source :
Chemistry (Weinheim an der Bergstrasse, Germany) [Chemistry] 2016 Dec 19; Vol. 22 (51), pp. 18559-18563. Date of Electronic Publication: 2016 Nov 11.
Publication Year :
2016

Abstract

Highly efficient, one-step synthesis of sulfur-containing heteroacenes was achieved through palladium-catalyzed C-S cross-coupling of bis-alkynes with thioacetate as hydrogen sulfide surrogate. Heteroacenes consisting of three, five, and seven fused aromatic rings were obtained in a single catalytic step by four-, six-, and eightfold C-S bond formation.<br /> (© 2016 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim.)

Details

Language :
English
ISSN :
1521-3765
Volume :
22
Issue :
51
Database :
MEDLINE
Journal :
Chemistry (Weinheim an der Bergstrasse, Germany)
Publication Type :
Academic Journal
Accession number :
27862441
Full Text :
https://doi.org/10.1002/chem.201603737