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Crystal structure of 3,9,9-trimethyl-2,3,3a,4,9,9a-hexa-hydro-1H-cyclo-penta[b]quinolin-4-ium chloride.
- Source :
-
Acta crystallographica. Section E, Crystallographic communications [Acta Crystallogr E Crystallogr Commun] 2015 Jun 27; Vol. 71 (Pt 7), pp. o525-6. Date of Electronic Publication: 2015 Jun 27 (Print Publication: 2015). - Publication Year :
- 2015
-
Abstract
- The title mol-ecular salt, C15H22N(+)·Cl(-), arose as an unexpected product of the reaction between aniline and melanol in the presence of HCl. The central heterocyclic ring has a half-chair conformation and the five-membered ring has an envelope conformation, with the C atom linked to the N atom as the flap. In the crystal, the ions are linked by N-H⋯Cl hydrogen bonds, generating chains propagating in the [100] direction. The crystal studied was a merohedral twin with a 0.64 (3):0.36 (3) domain ratio.
Details
- Language :
- English
- ISSN :
- 2056-9890
- Volume :
- 71
- Issue :
- Pt 7
- Database :
- MEDLINE
- Journal :
- Acta crystallographica. Section E, Crystallographic communications
- Publication Type :
- Academic Journal
- Accession number :
- 26279944
- Full Text :
- https://doi.org/10.1107/S2056989015011858