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Crystal structure of N-[(morpholin-4-yl)(thio-phen-2-yl)meth-yl]benzamide.

Authors :
Prabhu SA
Suresh M
Jameel AA
Padusha MS
Gunasekaran B
Source :
Acta crystallographica. Section E, Crystallographic communications [Acta Crystallogr E Crystallogr Commun] 2015 Jun 20; Vol. 71 (Pt 7), pp. o498-9. Date of Electronic Publication: 2015 Jun 20 (Print Publication: 2015).
Publication Year :
2015

Abstract

In the title compound, C16H18N2O2S, the morpholine ring adopts a chair conformation. The thio-phene ring makes a dihedral angle of 63.54 (14)° with the mean plane of the four C atoms [maximum deviation = 0.010 (3) Å] of the morpholine ring. The benzamide ring is disordered, with four C atoms occupying two sets of sites, with a refined occupancy ratio of 0.502 (4):0.498 (4). These two rings are inclined to one another by 85.2 (4)° and to the thio-phene ring by 72.7 (3) and 13.0 (3)° for the major and minor components, respectively. In the crystal, mol-ecules are linked via N-H⋯O hydrogen bonds, forming chains along [001].

Details

Language :
English
ISSN :
2056-9890
Volume :
71
Issue :
Pt 7
Database :
MEDLINE
Journal :
Acta crystallographica. Section E, Crystallographic communications
Publication Type :
Academic Journal
Accession number :
26279929
Full Text :
https://doi.org/10.1107/S2056989015011639