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An enantioselective total synthesis of Sch-725674.

Authors :
Ramakrishna K
Kaliappan KP
Source :
Organic & biomolecular chemistry [Org Biomol Chem] 2015 Jan 07; Vol. 13 (1), pp. 234-40.
Publication Year :
2015

Abstract

An enantioselective total synthesis of Sch-725674, a unique 14-membered macrolactone, has been accomplished in 13 steps. The step-wise dithiane alkylation served as a strategic step to assemble the upper and lower fragments of the molecule, whereas cross metathesis reaction, Yamaguchi macrolactonization and a substrate controlled stereoselective reduction are used as key steps to complete the total synthesis.

Details

Language :
English
ISSN :
1477-0539
Volume :
13
Issue :
1
Database :
MEDLINE
Journal :
Organic & biomolecular chemistry
Publication Type :
Academic Journal
Accession number :
25379975
Full Text :
https://doi.org/10.1039/c4ob02136c