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An oxidation-labile traceless linker for solid-phase synthesis.

Authors :
Stieber F
Grether U
Waldmann H
Source :
Angewandte Chemie (International ed. in English) [Angew Chem Int Ed Engl] 1999; Vol. 38 (8), pp. 1073-7.
Publication Year :
1999

Abstract

Traceless release of biaryls, acetylenes, alkenes, heterocycles, thioethers, and secondary amines from different solid supports can be achieved under very mild conditions by using a hydrazide group. This group, which is converted into an acyl diazene by oxidation and subsequently cleaved by a nucleophile (see scheme), is thus an attractive new linker for solid-phase synthesis and combinatorial chemistry.<br /> (Copyright © 1999 WILEY-VCH Verlag GmbH, Weinheim, Fed. Rep. of Germany.)

Details

Language :
English
ISSN :
1433-7851
Volume :
38
Issue :
8
Database :
MEDLINE
Journal :
Angewandte Chemie (International ed. in English)
Publication Type :
Academic Journal
Accession number :
25138498
Full Text :
https://doi.org/10.1002/(SICI)1521-3773(19990419)38:8<1073::AID-ANIE1073>3.0.CO;2-Y