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A new strategy to construct acyclic nucleosides via Ag(I)-catalyzed addition of pronucleophiles to 9-allenyl-9H-purines.

Authors :
Wei T
Xie MS
Qu GR
Niu HY
Guo HM
Source :
Organic letters [Org Lett] 2014 Feb 07; Vol. 16 (3), pp. 900-3. Date of Electronic Publication: 2014 Jan 17.
Publication Year :
2014

Abstract

A new strategy to construct acyclic nucleosides with diverse side chains was developed. With Ag(I) salts as catalysts, the hydrocarboxylation, hydroamination, and hydrocarbonation reactions proceeded well, affording acyclic nucleosides in good yields (41 examples, 60-98% yields). Meanwhile, these reactions exhibited high chemoselectivities and E-selectivities.

Details

Language :
English
ISSN :
1523-7052
Volume :
16
Issue :
3
Database :
MEDLINE
Journal :
Organic letters
Publication Type :
Academic Journal
Accession number :
24437554
Full Text :
https://doi.org/10.1021/ol4036566