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N,N'-Bis(phenyl-carbamo-thio-yl)benzene-1,3-dicarboxamide.

Authors :
Ngaini Z
Mohd Ariff MA
Wan Zullkiplee WS
Hussain H
Rosli MM
Source :
Acta crystallographica. Section E, Structure reports online [Acta Crystallogr Sect E Struct Rep Online] 2013 Aug 03; Vol. 69 (Pt 9), pp. o1374-5. Date of Electronic Publication: 2013 Aug 03 (Print Publication: 2013).
Publication Year :
2013

Abstract

The asymmetric unit of the title compound, C22H18N4O2S2, contains two mol-ecules. In one of them, the dihedral angles between the central benzene ring and the phenyl rings are 16.97 (8) and 20.97 (8)°, while the phenyl rings make a dihedral angle of 37.87 (8)°. In the other mol-ecule, the corresponding values are 34.92 (7), 53.90 (7) and 60.68 (8)°, respectively. In each mol-ecule, two intra-molecular N-H⋯O hydrogen bonds generate S(6) rings and a short C-H⋯S contact also occurs. In the crystal, N-H⋯S, N-H⋯O, C-H⋯O and C-H⋯S inter-actions link the mol-ecules into a three-dimensional network.

Details

Language :
English
ISSN :
1600-5368
Volume :
69
Issue :
Pt 9
Database :
MEDLINE
Journal :
Acta crystallographica. Section E, Structure reports online
Publication Type :
Academic Journal
Accession number :
24427019
Full Text :
https://doi.org/10.1107/S1600536813020163