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Tetra-butyl-ammonium 2-[2,5-dimethyl-3-(4-nitro-phen-yl)-2,3-dihydro-1,2,4-oxadiazo-lium-4-yl]nona-hydro-closo-deca-borate.

Authors :
Mindich AL
Pavlishchuk AV
Bokach NA
Starova GL
Zhizhin KY
Source :
Acta crystallographica. Section E, Structure reports online [Acta Crystallogr Sect E Struct Rep Online] 2012 Dec 01; Vol. 68 (Pt 12), pp. o3284-5. Date of Electronic Publication: 2012 Nov 03.
Publication Year :
2012

Abstract

The title ionic compound, C16H36N(+)·C10H20B10N3O3(-), consists of a tetra-butyl-ammonium cation and a closo-deca-borate cluster anion, which is bound to the substituted 2,3-dihydro-1,2,4-oxadiazole ring through a B-N bond [1.540 (2) Å]. The distances between connected B atoms in the deca-borate cluster range from 1.689 (2) to 1.844 (2) Å. The 2,3-dihydro-1,2,4-oxadiazole ring adopts an envelope conformation with the N atom as the flap atom.

Details

Language :
English
ISSN :
1600-5368
Volume :
68
Issue :
Pt 12
Database :
MEDLINE
Journal :
Acta crystallographica. Section E, Structure reports online
Publication Type :
Academic Journal
Accession number :
23468796
Full Text :
https://doi.org/10.1107/S1600536812044984