Back to Search Start Over

N-(2,3-Dimethyl-phen-yl)-2-nitro-benzene-sulfonamide.

Authors :
Chaithanya U
Foro S
Gowda BT
Source :
Acta crystallographica. Section E, Structure reports online [Acta Crystallogr Sect E Struct Rep Online] 2012 Nov 01; Vol. 68 (Pt 11), pp. o3188. Date of Electronic Publication: 2012 Oct 20.
Publication Year :
2012

Abstract

There are two independent mol-ecules in the asymmetric unit of the title compound, C(14)H(14)N(2)O(4)S. The N-H bonds are syn to the ortho-nitro groups in the sulfonyl benzene rings and anti to the methyl groups in the aniline benzene rings. The mol-ecules are twisted at the S-N bonds with torsion angles of -60.4 (3) and 58.8 (3)° in the two mol-ecules. The dihedral angles between the planes of the sulfonyl and the anilino benzene rings are 53.67 (8) and 56.99 (9)°. The amide H atoms of both mol-ecules are involved in an intra-molecular hydrogen bond, generating an S(7) motif. In the crystal, pairs of N-H⋯O(S) hydrogen bonds link like mol-ecules into inversion dimers.

Details

Language :
English
ISSN :
1600-5368
Volume :
68
Issue :
Pt 11
Database :
MEDLINE
Journal :
Acta crystallographica. Section E, Structure reports online
Publication Type :
Academic Journal
Accession number :
23284499
Full Text :
https://doi.org/10.1107/S1600536812042845