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Method for activation and recycling of trityl resins.

Authors :
Redwan IN
Grøtli M
Source :
The Journal of organic chemistry [J Org Chem] 2012 Aug 17; Vol. 77 (16), pp. 7071-5. Date of Electronic Publication: 2012 Aug 06.
Publication Year :
2012

Abstract

This note describes a rapid and mild strategy for the loading of alcohols and anilines onto a polystyrene triphenylmethyl (trityl) resin. High loadings were obtained in a matter of minutes by treating resin-bound trityl chloride with triethyloxonium tetrafluoroborate followed by alcohols or anilines. Yields were comparable or better than known literature methods. Recycling of the recovered resin was also possible using the developed method.

Details

Language :
English
ISSN :
1520-6904
Volume :
77
Issue :
16
Database :
MEDLINE
Journal :
The Journal of organic chemistry
Publication Type :
Academic Journal
Accession number :
22809057
Full Text :
https://doi.org/10.1021/jo300598d