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Low temperature solventless synthesis and characterization of Ni and Fe magnetic nanoparticles.

Authors :
Seinberg L
Yamamoto S
Gallage R
Tsujimoto M
Kobayashi Y
Isoda S
Takano M
Kageyama H
Source :
Chemical communications (Cambridge, England) [Chem Commun (Camb)] 2012 Aug 25; Vol. 48 (66), pp. 8237-9. Date of Electronic Publication: 2012 Jul 11.
Publication Year :
2012

Abstract

We have successfully implemented a facile, one-pot solventless synthesis procedure starting from acetylacetonate salts and CaH(2) to obtain carbon-coated ferromagnetic metallic Ni and Fe nanoparticles at low temperature. The use of CaH(2) as a reductant drastically reduces reaction temperature down to 140 °C.

Details

Language :
English
ISSN :
1364-548X
Volume :
48
Issue :
66
Database :
MEDLINE
Journal :
Chemical communications (Cambridge, England)
Publication Type :
Academic Journal
Accession number :
22785355
Full Text :
https://doi.org/10.1039/c2cc33830k