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A triclinic polymorph of (E)-2-(1-hy-droxy-3-phenyl-prop-2-en-1-yl-idene)-4,5-dimeth-oxy-cyclo-pent-4-ene-1,3-dione.
- Source :
-
Acta crystallographica. Section E, Structure reports online [Acta Crystallogr Sect E Struct Rep Online] 2012 Feb 01; Vol. 68 (Pt 2), pp. o453. Date of Electronic Publication: 2012 Jan 18. - Publication Year :
- 2012
-
Abstract
- The title compound, C(16)H(14)O(5), is a triclinic polymorph of a previously reported monoclinic structure [Hosseinzadeh et al. (2011 ▶). Acta Cryst. E67, o1544]. The mol-ecule is roughly planar, the r.m.s. deviation from the least-squares plane of all non-H atoms being 0.092 Å. In the crystal, adjacent mol-ecules are linked through C-H⋯O hydrogen bonds into an infinite two-dimensional network parallel to (011). The layers are further connected via C-H⋯π inter-actions, forming a three-dimensional structure. Intra-molecular O-H⋯O and C-H⋯O hydrogen bonds are also observed.
Details
- Language :
- English
- ISSN :
- 1600-5368
- Volume :
- 68
- Issue :
- Pt 2
- Database :
- MEDLINE
- Journal :
- Acta crystallographica. Section E, Structure reports online
- Publication Type :
- Academic Journal
- Accession number :
- 22347064
- Full Text :
- https://doi.org/10.1107/S1600536812001043