Complete assignment of NMR data of 22 phenyl-1H-pyrazoles' derivatives.

Authors :: de Oliveira AL
Alves de Oliveira CH
Mairink LM
Pazini F
Menegatti R
Lião LM
Source :: Magnetic resonance in chemistry : MRC [Magn Reson Chem] 2011 Aug; Vol. 49 (8), pp. 537-42. Date of Electronic Publication: 2011 Jul 14.
Publication Year :: 2011
Abstract: Complete assignment of (1)H and (13)C NMR chemical shifts and J((1)H/(1)H and (1)H/(19)F) coupling constants for 22 1-phenyl-1H-pyrazoles' derivates were performed using the concerted application of (1)H 1D and (1)H, (13)C 2D gs-HSQC and gs-HMBC experiments. All 1-phenyl-1H-pyrazoles' derivatives were synthesized as described by Finar and co-workers. The formylated 1-phenyl-1H-pyrazoles' derivatives were performed under Duff's conditions.<br /> (Copyright © 2011 John Wiley & Sons, Ltd.)