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3-Fluoro-benzoic acid-4-acetyl-pyridine (1/1) at 100 K.

Authors :
Craig GA
Thomas LH
Adam MS
Ballantyne A
Cairns A
Cairns SC
Copeland G
Harris C
McCalmont E
McTaggart R
Martin AR
Palmer S
Quail J
Saxby H
Sneddon DJ
Stewart G
Thomson N
Whyte A
Wilson CC
Parkin A
Source :
Acta crystallographica. Section E, Structure reports online [Acta Crystallogr Sect E Struct Rep Online] 2009 Jan 23; Vol. 65 (Pt 2), pp. o380. Date of Electronic Publication: 2009 Jan 23.
Publication Year :
2009

Abstract

In the title compound, C(7)H(5)FO(2)·C(7)H(7)NO, a moderate-strength hydrogen bond is formed between the carboxyl group of one mol-ecule and the pyridine N atom of the other. The benzoic acid mol-ecule is observed to be disordered over two positions with the second orientation only 4% occupied. This disorder is also reflected in the presence of diffuse scattering in the diffraction pattern.

Details

Language :
English
ISSN :
1600-5368
Volume :
65
Issue :
Pt 2
Database :
MEDLINE
Journal :
Acta crystallographica. Section E, Structure reports online
Publication Type :
Academic Journal
Accession number :
21581976
Full Text :
https://doi.org/10.1107/S1600536809002396