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Synthesis of novel N-hydroxy heterocycles via intramolecular reductive cyclization of diketoximes by NaBH3CN.

Authors :
Nagaraj M
Boominathan M
Muthusubramanian S
Bhuvanesh N
Source :
Organic & biomolecular chemistry [Org Biomol Chem] 2011 Jun 21; Vol. 9 (12), pp. 4642-52. Date of Electronic Publication: 2011 Apr 28.
Publication Year :
2011

Abstract

A simple and efficient protocol for the construction of substituted piperazines, piperidines, thiomorpholines, decahydroquinolines, perhydrocyclopenta[b]pyridine, and pyrrolidines bearing N-hydroxy substituents through intramolecular reductive cyclization of diketoximes using sodium cyanoborohydride is described.

Details

Language :
English
ISSN :
1477-0539
Volume :
9
Issue :
12
Database :
MEDLINE
Journal :
Organic & biomolecular chemistry
Publication Type :
Academic Journal
Accession number :
21526255
Full Text :
https://doi.org/10.1039/c1ob05232b