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1-Methyl-2-(4-methyl-phen-yl)-4-morpholinopyridazine-3,6(1H,2H)-dione.

Authors :
Gzella A
Melzer E
Kaczmarek MS
Woźniak Z
Source :
Acta crystallographica. Section E, Structure reports online [Acta Crystallogr Sect E Struct Rep Online] 2008 Jan 11; Vol. 64 (Pt 2), pp. o435. Date of Electronic Publication: 2008 Jan 11.
Publication Year :
2008

Abstract

The structure analysis of the title compound, C(16)H(19)N(3)O(3), has been undertaken in order to facilitate the inter-pretation of (1)H and (13)C NMR data and to determine the position of the morpholine residue in this nucleophilic substitution product. The main result is that the morpholine group, with a chair conformation, is connected at the 4-position of the pyridazine ring. The benzene and pyridazine rings make a dihedral angle of 62.17 (5)°. Mol-ecules are linked into a two-dimensional network by non-classical C-H⋯O hydrogen bonds, in which O atoms serve as double or triple acceptors.

Details

Language :
English
ISSN :
1600-5368
Volume :
64
Issue :
Pt 2
Database :
MEDLINE
Journal :
Acta crystallographica. Section E, Structure reports online
Publication Type :
Academic Journal
Accession number :
21201462
Full Text :
https://doi.org/10.1107/S1600536808000111