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Preparation of Sr7Mn4O13F2 by the topotactic reduction and subsequent fluorination of Sr7Mn4O15.

Authors :
Saratovsky I
Lockett MA
Rees NH
Hayward MA
Source :
Inorganic chemistry [Inorg Chem] 2008 Jun 16; Vol. 47 (12), pp. 5212-7. Date of Electronic Publication: 2008 May 10.
Publication Year :
2008

Abstract

The topotactic reduction and subsequent fluorination of Sr7Mn4O15 yields a phase of composition Sr7Mn4O13F2. Characterization of this phase utilizing powder neutron diffraction and 19F NMR shows that the fluoride ions are located on a single anion site, the same crystallographic site that is vacant in the reduced intermediate Sr7Mn4O13.

Details

Language :
English
ISSN :
0020-1669
Volume :
47
Issue :
12
Database :
MEDLINE
Journal :
Inorganic chemistry
Publication Type :
Academic Journal
Accession number :
18470979
Full Text :
https://doi.org/10.1021/ic800066g