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Transamination chemistry of sodium TMP-zincate: synthesis and crystal structure of a chiral amidozincate.

Authors :
Armstrong DR
Clegg W
Dale SH
García-Alvarez J
Harrington RW
Hevia E
Honeyman GW
Kennedy AR
Mulvey RE
O'Hara CT
Source :
Chemical communications (Cambridge, England) [Chem Commun (Camb)] 2008 Jan 14 (2), pp. 187-9. Date of Electronic Publication: 2007 Nov 13.
Publication Year :
2008

Abstract

In a new type of reactivity for sodium TMP-zincate [(TMEDA)NaZn((t)Bu)(2)(TMP)] (1), transamination reactions with the amines diisopropylamine, DA(H), hexamethyldisilazane, HMDS(H) and chiral (R)-N-benzyl-alpha-methylbenzylamine have produced new sodium amido-di-tert-butyl zincates (all structurally characterised) with concomitant loss of TMP(H).

Details

Language :
English
ISSN :
1359-7345
Issue :
2
Database :
MEDLINE
Journal :
Chemical communications (Cambridge, England)
Publication Type :
Academic Journal
Accession number :
18092082
Full Text :
https://doi.org/10.1039/b713987j