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Synthesis and characterization of aluminum-containing tin(IV) heterobimetallic sulfides.
- Source :
-
Inorganic chemistry [Inorg Chem] 2006 Apr 17; Vol. 45 (8), pp. 3312-5. - Publication Year :
- 2006
-
Abstract
- Three novel aluminum-containing tin(IV) heterobimetallic sulfides are reported. The reaction of [LAl(SLi)2(THF)2]2 (1) [L = HC(CMeNAr)2, Ar = 2,6-iPr2C6H3] with Ph2SnCl2, Me2SnCl2, and SnCl4 in THF respectively afforded LAl(mu-S)2SnPh2 (2), LAl(mu-S)2SnMe2 (3), and LAl(mu-S)2Sn(mu-S)2AlL (4) in moderate yields. Compounds 2, 3, and 4 were characterized by elemental analysis, NMR, electron-impact mass spectrometry, and single-crystal X-ray structural analysis.
Details
- Language :
- English
- ISSN :
- 0020-1669
- Volume :
- 45
- Issue :
- 8
- Database :
- MEDLINE
- Journal :
- Inorganic chemistry
- Publication Type :
- Academic Journal
- Accession number :
- 16602790
- Full Text :
- https://doi.org/10.1021/ic052139m