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Imaging columns of the light elements carbon, nitrogen and oxygen with sub Angstrom resolution.

Authors :
Kisielowski C
Hetherington CJ
Wang YC
Kilaas R
O'Keefe MA
Thust A
Source :
Ultramicroscopy [Ultramicroscopy] 2001 Nov; Vol. 89 (4), pp. 243-63.
Publication Year :
2001

Abstract

It is reported that lattice imaging with a 300 kV field emission microscope in combination with numerical reconstruction procedures can be used to reach an interpretable resolution of about 80 pm for the first time. A retrieval of the electron exit wave from focal series allows for the resolution of single atomic columns of the light elements carbon, nitrogen, and oxygen at a projected nearest neighbor spacing down to 85 pm. Lens aberrations are corrected on-line during the experiment and by hardware such that resulting image distortions are below 80 pm. Consequently, the imaging can be aberration-free to this extent. The resolution enhancement results from increased electrical and mechanical stability of the instrument coupled with a low spherical aberration coefficient of 0.595 + 0.005 mm.

Details

Language :
English
ISSN :
0304-3991
Volume :
89
Issue :
4
Database :
MEDLINE
Journal :
Ultramicroscopy
Publication Type :
Academic Journal
Accession number :
11766981
Full Text :
https://doi.org/10.1016/s0304-3991(01)00090-0