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Dipolar Assisted Assignment Protocol (DAAP) for MAS solid-state NMR of rotationally aligned membrane proteins in phospholipid bilayers.

Authors :
Das, Bibhuti B.
Zhang, Hua
Opella, Stanley J.
Source :
Journal of Magnetic Resonance. May2014, Vol. 242, p224-232. 9p.
Publication Year :
2014

Abstract

Highlights: [•] Correct angular restraints are obtained for rotationally aligned Vpu TM. [•] Pulse sequences for a dipolar assisted assignment protocol are described. [•] Pulse sequences that measure chemical shifts and dipolar frequencies are described. [•] Chemical shift and dipolar frequency correlation provides high resolution. [Copyright &y& Elsevier]

Details

Language :
English
ISSN :
10907807
Volume :
242
Database :
Academic Search Index
Journal :
Journal of Magnetic Resonance
Publication Type :
Academic Journal
Accession number :
95783969
Full Text :
https://doi.org/10.1016/j.jmr.2014.02.018