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Synthesis of Mo(PMe3)6 and trans-Mo(PMe3)4(E)2 (E = S, Se, Te): The first series of terminal...

Authors :
Murphy, Vincent J.
Parkin, Gerard
Source :
Journal of the American Chemical Society. 3/29/95, Vol. 117 Issue 12, p3522. 7p. 6 Diagrams, 10 Charts, 1 Graph.
Publication Year :
1995

Abstract

Describes the synthesis of Mo(PMe3)6 and the thermodynamic details of the equilibrium of Mo(PMe3)6 with its cyclometalated derivative Mo(PMe3)4(eta2-CH2PMe2)H and PMe3. Mechanism of synthesis; Equilibration thermodynamics; Use of the trimethylphosphine complexes in the syntheses of terminal sulfido, selenido, and tellurido complexes of molybdenum.

Details

Language :
English
ISSN :
00027863
Volume :
117
Issue :
12
Database :
Academic Search Index
Journal :
Journal of the American Chemical Society
Publication Type :
Academic Journal
Accession number :
9507123508
Full Text :
https://doi.org/10.1021/ja00117a021