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A benzene-thermal synthesis of powdered cubic zirconium nitride
- Source :
-
Materials Letters . Mar2003, Vol. 57 Issue 11, p1679. 4p. - Publication Year :
- 2003
-
Abstract
- Powdered zirconium nitride (ZrN) has been prepared via a benzene-thermal synthesis via the reaction of anhydrous zirconium tetrachloride (ZrCl4) and lithium nitride (Li3N) at a temperature of 380–400 °C. The product was analyzed by X-ray photoelectron spectroscopy (XPS), and the results show the mole ratio of Zr/N is 1:0.87. X-ray diffraction (XRD) pattern can be indexed to the cubic cell of ZrN with the lattice constant a=4.5675 A˚. Transmission electron microscope (TEM) images indicate that average particle size is about 180 nm in diameter. [Copyright &y& Elsevier]
- Subjects :
- *ZIRCONIUM
*PHOTOELECTRON spectroscopy
Subjects
Details
- Language :
- English
- ISSN :
- 0167577X
- Volume :
- 57
- Issue :
- 11
- Database :
- Academic Search Index
- Journal :
- Materials Letters
- Publication Type :
- Academic Journal
- Accession number :
- 9144606
- Full Text :
- https://doi.org/10.1016/S0167-577X(02)01051-0