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An improved synthesis, characterization, and X-ray studies of 5-tert-butyl-3-nitrophthalonitrile.
- Source :
-
Tetrahedron Letters: International Organ for the Rapid Publication of Preliminary Communications in Organic Chemistry . Jul2013, Vol. 54 Issue 29, p3816-3818. 3p. - Publication Year :
- 2013
-
Abstract
- Abstract: An improved six-step synthesis of 5-tert-butyl-3-nitrophthalonitrile (1) is described. The title compound and all the intermediates are fully characterized spectroscopically (FT–IR, 1H NMR, 13C NMR, MS). In addition, single-crystal X-ray diffraction further confirmed the structure of the title compound. [Copyright &y& Elsevier]
Details
- Language :
- English
- ISSN :
- 00404039
- Volume :
- 54
- Issue :
- 29
- Database :
- Academic Search Index
- Journal :
- Tetrahedron Letters: International Organ for the Rapid Publication of Preliminary Communications in Organic Chemistry
- Publication Type :
- Academic Journal
- Accession number :
- 89117273
- Full Text :
- https://doi.org/10.1016/j.tetlet.2013.05.045