An improved synthesis, characterization, and X-ray studies of 5-tert-butyl-3-nitrophthalonitrile.

Authors :: Łapok, Łukasz
Siudak, Alicja
Nowakowska, Maria
Source :: Tetrahedron Letters: International Organ for the Rapid Publication of Preliminary Communications in Organic Chemistry. Jul2013, Vol. 54 Issue 29, p3816-3818. 3p.
Publication Year :: 2013
Abstract: Abstract: An improved six-step synthesis of 5-tert-butyl-3-nitrophthalonitrile (1) is described. The title compound and all the intermediates are fully characterized spectroscopically (FT–IR, 1H NMR, 13C NMR, MS). In addition, single-crystal X-ray diffraction further confirmed the structure of the title compound. [Copyright &y& Elsevier]

Subjects :: *BENZENEDICARBONITRILE
*NUCLEAR magnetic resonance spectroscopy
*MOLECULAR structure
*ADDITION reactions
*X-ray diffraction
*INTERMEDIATES (Chemistry)
*ORGANIC synthesis

Language :: English
ISSN :: 00404039
Volume :: 54
Issue :: 29
Database :: Academic Search Index
Journal :: Tetrahedron Letters: International Organ for the Rapid Publication of Preliminary Communications in Organic Chemistry
Publication Type :: Academic Journal
Accession number :: 89117273
Full Text :: https://doi.org/10.1016/j.tetlet.2013.05.045

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