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Synthesis and characterization of Cu, Ag and Au dendrimer-encapsulated nanoparticles and their application in the reduction of 4-nitrophenol to 4-aminophenol
- Source :
-
Journal of Colloid & Interface Science . Jan2013, Vol. 389 Issue 1, p260-267. 8p. - Publication Year :
- 2013
-
Abstract
- Abstract: Here, we report on the synthesis, characterization and catalytic evaluation of Cu, Ag and Au dendrimer encapsulated nanoparticles (DENs). Generations 4–6 of PAMAM-OH and PAMAM-NH2 were used as templating agents for the synthesis of Cu and Ag-DENs respectively. Generation 4 PAMAM-NH2 dendrimers were used for the synthesis of Au-DENs. These prepared DENs were characterized using UV visible (UV–vis) spectroscopy as well as a high resolution transmission electron microscopy (HRTEM). The catalytic activity of these DENs was evaluated on the reduction of 4-nitrophenol (4-NP) to 4-aminophenol (4-AMP) by sodium borohydride (NaBH4). The reaction was monitored by UV–vis spectroscopy at λ 400nm. These prepared DENs were found to exhibit good activity for this reduction reaction. [Copyright &y& Elsevier]
Details
- Language :
- English
- ISSN :
- 00219797
- Volume :
- 389
- Issue :
- 1
- Database :
- Academic Search Index
- Journal :
- Journal of Colloid & Interface Science
- Publication Type :
- Academic Journal
- Accession number :
- 82897235
- Full Text :
- https://doi.org/10.1016/j.jcis.2012.09.012