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Microwave-Assisted and Iodine-Catalyzed Synthesis of Dihydropyrimidin-2-thiones via Biginelli Reaction Under Solvent-Free Conditions.
- Source :
-
Synthetic Communications . Jan2013, Vol. 43 Issue 1, p139-146. 8p. 3 Diagrams, 2 Charts. - Publication Year :
- 2013
-
Abstract
- Microwave-assisted synthesis of 3,4-dihydropyrimidin-2-thiones via Biginelli reaction from aldehydes, acetoacetates, and thiourea in the presence of iodine under solvent-free conditions has been accomplished in good yields and purity without chromatographic separation. [ABSTRACT FROM PUBLISHER]
Details
- Language :
- English
- ISSN :
- 00397911
- Volume :
- 43
- Issue :
- 1
- Database :
- Academic Search Index
- Journal :
- Synthetic Communications
- Publication Type :
- Academic Journal
- Accession number :
- 79723009
- Full Text :
- https://doi.org/10.1080/00397911.2011.593289