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Bright-field scanning confocal electron microscopy using a double aberration-corrected transmission electron microscope

Authors :
Wang, Peng
Behan, Gavin
Kirkland, Angus I.
Nellist, Peter D.
Cosgriff, Eireann C.
D’Alfonso, Adrian J.
Morgan, Andrew J.
Allen, Leslie J.
Hashimoto, Ayako
Takeguchi, Masaki
Mitsuishi, Kazutaka
Shimojo, Masayuki
Source :
Ultramicroscopy. Jun2011, Vol. 111 Issue 7, p877-886. 10p.
Publication Year :
2011

Abstract

Abstract: Scanning confocal electron microscopy (SCEM) offers a mechanism for three-dimensional imaging of materials, which makes use of the reduced depth of field in an aberration-corrected transmission electron microscope. The simplest configuration of SCEM is the bright-field mode. In this paper we present experimental data and simulations showing the form of bright-field SCEM images. We show that the depth dependence of the three-dimensional image can be explained in terms of two-dimensional images formed in the detector plane. For a crystalline sample, this so-called probe image is shown to be similar to a conventional diffraction pattern. Experimental results and simulations show how the diffracted probes in this image are elongated in thicker crystals and the use of this elongation to estimate sample thickness is explored. [Copyright &y& Elsevier]

Details

Language :
English
ISSN :
03043991
Volume :
111
Issue :
7
Database :
Academic Search Index
Journal :
Ultramicroscopy
Publication Type :
Academic Journal
Accession number :
61258419
Full Text :
https://doi.org/10.1016/j.ultramic.2010.10.012