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Addition of allyl bromide to phenylacetylene catalyzed by palladium on alumina and its application to a continuous flow synthesis.
- Source :
-
Research on Chemical Intermediates . 2009, Vol. 35 Issue 8/9, p1053-1057. 5p. 2 Diagrams, 1 Chart. - Publication Year :
- 2009
-
Abstract
- The reaction of allyl bromide with phenylacetylene catalyzed by Pd/Al2O3 pellets and Pd/C powder was investigated. Bromoallylation of phenylacetylene took place to give a regioisomeric mixture of 1-bromo-substituted 1,4-dienes. The bromoallylation of phenylacetylene was successfully applied to a continuous flow synthesis using a stainless steel made column packed with Pd/Al2O3 pellets. [ABSTRACT FROM AUTHOR]
- Subjects :
- *BROMIDES
*PALLADIUM
*CATALYSIS
*STAINLESS steel
*STEEL alloys
*BROMINE compounds
Subjects
Details
- Language :
- English
- ISSN :
- 09226168
- Volume :
- 35
- Issue :
- 8/9
- Database :
- Academic Search Index
- Journal :
- Research on Chemical Intermediates
- Publication Type :
- Academic Journal
- Accession number :
- 47010684
- Full Text :
- https://doi.org/10.1007/s11164-009-0069-x