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Chlorination of Aniline and Methyl Carbanilate by N-Chlorosuccinimide and Synthesis of 1,3,5-Trichlorobenzene.
- Source :
-
Synthetic Communications . 2009, Vol. 39 Issue 6, p1100-1108. 9p. 4 Diagrams. - Publication Year :
- 2009
-
Abstract
- Aniline undergoes regioselective trichlorination by N-chlorosuccinimide (NCS) in acetonitrile in good yield. The product 2,4,6-trichoroaniline was converted into 1,3,5-trichlorobenzene by reduction of its diazonium salt. Reaction of the methyl carbamate of aniline with NCS gave only the 2,4-dichlorophenyl carbamate. [ABSTRACT FROM AUTHOR]
- Subjects :
- *CHLORINATION
*ANILINE
*AROMATIC amines
*DIPHENYLAMINE
*SUCCINIMIDES
Subjects
Details
- Language :
- English
- ISSN :
- 00397911
- Volume :
- 39
- Issue :
- 6
- Database :
- Academic Search Index
- Journal :
- Synthetic Communications
- Publication Type :
- Academic Journal
- Accession number :
- 36635361
- Full Text :
- https://doi.org/10.1080/00397910802499542