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Synthesis and NMR experiments of (4,5,6-13C)-deoxymannojirimycin. A new entry to 13C-labeled glycosidase inhibitors
- Source :
-
Carbohydrate Research . Sep2007, Vol. 342 Issue 12/13, p1805-1812. 8p. - Publication Year :
- 2007
-
Abstract
- Abstract: The synthesis of (4,5,6-13C)-deoxymannojirimycin is described. The route employed is based on Sharpless asymmetric epoxidation of (1,2,3-13C)(E)-2,4-pentadien-1-ol and uses ring-closing metathesis as a key step. The labeled compound may be easily used for protein-binding experiments using NMR spectroscopic methods. [Copyright &y& Elsevier]
Details
- Language :
- English
- ISSN :
- 00086215
- Volume :
- 342
- Issue :
- 12/13
- Database :
- Academic Search Index
- Journal :
- Carbohydrate Research
- Publication Type :
- Academic Journal
- Accession number :
- 25827650
- Full Text :
- https://doi.org/10.1016/j.carres.2007.04.018