Pinhole small‐angle neutron scattering based approach for desmearing slit ultra‐small‐angle neutron scattering data.

Presented here is an effective approach to desmearing slit ultra‐small‐angle neutron scattering (USANS) data, based on complementary small‐angle neutron scattering (SANS) measurements, leading to a seamless merging of these data sets. The study focuses on the methodological aspects of desmearing USANS data, which can then be presented in the conventional manner of SANS, enabling a broader pool of data analysis methods. The key innovation lies in the use of smeared SANS data for extrapolating slit USANS, offering a self‐consistent integrand function for desmearing with Lake's iterative method. The proposed approach is validated through experimental data on porous anodized aluminium oxide membranes, showcasing its applicability and benefits. The findings emphasize the importance of accurate desmearing for merging USANS and SANS data in the crossover q region, which is particularly crucial for complex scattering patterns. [ABSTRACT FROM AUTHOR]