Effect of hollow glass microspheres on transverse properties of carbon fiber reinforced epoxy composites.

Highlights Hollow glass microsphere (HGM)—based composites are gaining popularity in materials research due to their ability in altering material characteristics drastically. The current study investigates HGMs filled carbon fiber reinforced epoxy (CE) composites on transverse properties, aiming for aerospace and defense applications mainly in composite pressure vessels. Unidirectional laminates of Carbon/Epoxy with varying HGM percentages (0.2, 0.4, 0.6, 0.8, 1.0 wt. %) were wounded onto a flat‐plate mandrel using a 4‐axis filament winder, along with a baseline sample without HGM for comparison. The glass transition temperature (Tg) and thermal stability were analyzed by carrying out dynamic mechanical analysis and thermogravimetric analysis. The fracture mechanism of the samples loaded under tension was investigated using FESEM. Experimental results indicate reduction in density with increase in HGM content, up to 0.4% HGM there is increase in transverse tensile strength of 25% compared to baseline and further increase in HGM content, decrease trend is observed. 30% decrease in transverse compressive strength is observed compared from baseline to 1.0 wt. % of HGM. No significant change was noticed in the thermal stability and Tg on introduction of HGM. Microscopy images of fractured samples revealed effective physical interaction and dispersion of the HGM within the matrix. Transverse mechanical properties are tested to know the influence of HGM filler on filament wound composites. Density of the composite decreases with increase in HGM content. Thermal stability and Tg shows less change on introduction of HGM in composites. [ABSTRACT FROM AUTHOR]