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(E)-1-(4-Methoxyphenyl)-5-methyl-4-(1-phenyl-4-((2-(2,4,6-trichlorophenyl)hydrazineylidene)methyl)-1 H -pyrazol-3-yl)-1 H -1,2,3-triazole.

Authors :
Abdel-Wahab, Bakr F.
Mohamed, Hanan A.
Kariuki, Benson M.
El-Hiti, Gamal A.
Source :
Molbank. Jun2024, Vol. 2024 Issue 2, pM1798. 7p.
Publication Year :
2024

Abstract

The reaction of equimolar quantities of 3-(1-(4-methoxyphenyl)-5-methyl-1H-1,2,3-triazol-4-yl)-1-phenyl-1H-pyrazole-4-carbaldehyde and (2,4,6-trichlorophenyl)hydrazine in ethanol containing concentrated hydrochloric acid (0.2 mL; 37%) as a catalyst under reflux for 2 h yielded 1-(1-(benzofuran-2-yl)ethylidene)-2-(2,4,6-trichlorophenyl)hydrazine. The crude produced was purified by crystallization using dimethylformamide to provide the title heterocycle in a 95% yield. The structure of the newly synthesized heterocycle was confirmed through X-ray diffraction and spectral analyses. [ABSTRACT FROM AUTHOR]

Details

Language :
English
ISSN :
14228599
Volume :
2024
Issue :
2
Database :
Academic Search Index
Journal :
Molbank
Publication Type :
Academic Journal
Accession number :
178185663
Full Text :
https://doi.org/10.3390/M1798