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Scanning ex situ solid-state magnetic resonance imaging on polymeric films using a static magnetic field gradient by an electromagnet.

Authors :
Kawabata, Natsuki
Asakawa, Naoki
Source :
Review of Scientific Instruments. Apr2024, Vol. 95 Issue 4, p1-8. 8p.
Publication Year :
2024

Abstract

A new technique for ex situ solid-state nuclear magnetic resonance imaging of polymeric films has been developed. This method uses the static magnetic field gradient generated by a water-cooled copper electromagnet. The imaging process involves scanning the sample in the plane of the film under a static magnetic field gradient. Two-dimensional (2D) 19F MRI measurements are attempted, where the fast Fourier transform (FFT) spectra of the second half of a Hahn echo peak is used for the depth (X-axis) direction, and the sample film is mechanically moved for the Y-axis, which is in-plane with respect to the film surface and normal to the inter-magnetic-pole line (Z-axis). The sample is a poly(tetrafluoroethylene) [PTFE] film with carved stripes on its surface. Furthermore, three-dimensional (3D) measurements of the film surface and thickness orientations were also performed for an analogous PTFE film. For 2D profiling on the film surface, 2D sample-moving was used. For depth profiling, FFT spectrum analysis was undertaken for each voxel situated at a specific (Y, Z) coordinate within the film. As a result, a 3D image of the sample and its corresponding geometry were obtained, although the scanning area was restricted to a part of the sample. Finally, numerical simulations of the spatial distribution of the static magnetic field were performed to confirm the validity of the present method. [ABSTRACT FROM AUTHOR]

Details

Language :
English
ISSN :
00346748
Volume :
95
Issue :
4
Database :
Academic Search Index
Journal :
Review of Scientific Instruments
Publication Type :
Academic Journal
Accession number :
177184013
Full Text :
https://doi.org/10.1063/5.0188529