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Physical, chemical, and thermal properties of chia and okra mucilages.

Authors :
Santos, Francislaine Suelia dos
Figueirêdo, Rossana Maria Feitosa de
de Melo Queiroz, Alexandre José
Paiva, Yaroslávia Ferreira
Araújo, Auryclennedy Calou de
Lima, Thalis Leandro Bezerra de
de Brito Araújo Carvalho, Ana Júlia
dos Santos Lima, Marcos
Macedo, Antônio Daniel Buriti de
Campos, Ana Regina Nascimento
Source :
Journal of Thermal Analysis & Calorimetry. Jul2023, Vol. 148 Issue 14, p7463-7475. 13p.
Publication Year :
2023

Abstract

The present study aims to investigate the physical, chemical, and thermal properties of chia (CM) and okra (OM) mucilages powders. The mucilages were extracted and dehydrated at 70 °C; then they were evaluated for the profile of total phenolic compounds and mineral profile, colorimetric parameters, morphology by scanning electron microscopy (SEM), infrared by fourier transform (FTIR), X-ray diffraction (XRD), and thermal properties by differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA/DTG). It was found that OM had higher amounts of total phenolic compounds, mainly flavonols, with a predominance of quercetin 3-glucoside. On the other hand, CM had the highest content of flavonoids, the most significant being catechin. CM had the highest mineral content, being surpassed by okra mucilage in terms of calcium and copper. The OM had the highest luminosity, with values tending toward yellow and green tones, while the CM was darker and presented yellow and red tones. The mucilages presented morphologically irregular particles with different sizes and shapes, with an amorphous structure. The FTIR showed the bands of the main components, indicating that the mucilages are constituted mainly by polysaccharides (OM), pectins, and soluble proteins (CM). The DSC showed sharp endothermic peaks, indicating greater uniformity and purity of the samples. The thermogravimetric curves and their derivatives showed the greatest mass loss in the second evaluation phase for both materials, followed by the carbonization of organic matter and the formation of fixed mineral residue. The study revealed that mucilages have distinct characteristics, but with excellent properties, which offers great potential as a raw material for industry. [ABSTRACT FROM AUTHOR]

Details

Language :
English
ISSN :
13886150
Volume :
148
Issue :
14
Database :
Academic Search Index
Journal :
Journal of Thermal Analysis & Calorimetry
Publication Type :
Academic Journal
Accession number :
164580249
Full Text :
https://doi.org/10.1007/s10973-023-12179-0