CuCe-Ferrite/TiO2 Nanocomposite as an Efficient Magnetically Separable Photocatalyst for Dye Pollutants Decolorization.

In this work, a magnetically separated photocatalyst with great efficiency CuCe-Ferrite/TiO2 composite was prepared and characterized by X-ray diffraction (XRD), UV–Vis spectrophotometry, Fourier transformer infra-red spectroscopy (FTIR), field emission scanning electron microscopy (FE-SEM), high resolution transmission electron microscopy (HR-TEM), energy dispersive X-ray spectroscopy (EDX) and vibrating sample magnetometer (VSM). Single-phase cubic spinel was formed by calcining the prepared sample at a temperature of 550 °C, according to the results. Different concentrations of reactive red 250 (RR250) dye photodegradation was evaluated using different doses of CuCe-ferrite/ TiO2 and TiO2 NPs. Higher efficiency of RR250 photodegradation up to 100% was obtained using CuCe-ferrite/ TiO2. The photodegradation efficiency was confirmed using chemical oxygen demand (COD) test of both treated and untreated samples. The oxidation process was mostly mediated by photogenerated .O2− according to scavenger test results. The catalyst possess higher photodegradation efficiency even after regeneration for ten times. [ABSTRACT FROM AUTHOR]